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Precision and accuracies fell within acceptable limits (20 % for LLOQ and 15 %) for both intra- and inter-day analyses for all compounds except acetaldehyde which had inter-day variability of ≤25 %. The linearity of the method was established over the range 0.2–100 mg/L (R Google Scholar, Christophersen AS, Gjerde H, Bjorneboe A, Sakshaug J, Morland J (1990) Screening for drug use among Norwegian drivers suspected of driving under influence of alcohol or drugs. Int J Toxicol 24:69–77, Article  Ethanol production, purification, and analysis techniques: a review Abstract World ethanol production rose to nearly 13.5 billion gallon in 2006. By continuing you agree to the use of cookies. Int J Toxicol 22:377–380, Whittaker A, Currie AE, Turner MA, Field DJ, Mulla H, Pandya HC (2009) Toxic additives in medication for preterm infants. Google Scholar, Zuba D, Piekoszewski W, Pach J, Winnik L, Parczewski A (2002) Concentration of ethanol and other volatile compounds in the blood of acutely poisoned alcoholics. volume 405, pages4139–4147(2013)Cite this article. Anal Chim Acta 522:163–168, Zuba D, Parczewski A, Reichenbacher M (2002) Optimization of solid-phase microextraction conditions for gas chromatographic determination of ethanol and other volatile compounds in blood. Analysis of Ethanol in the Whole Blood 387 GC/MS has also been utilized for determination of al-cohol concentration in serum. The method used for sample preparation was simple. Am J Clin Pathol 74:747–750, CAS  ► Prediction of ethanol content of meals cooked with alcoholic drinks. ► Potential hazards of intake of meals cooked with alcoholic drinks by ethanol sensible individuals. Anal Chem 64:1021–1029, Lewis SJ, Zuccolo L, Davey Smith G, Macleod J, Rodriguez S, Draper ES, Barrow M, Alati R, Sayal K, Ring S, Golding J, Gray R (2012) Fetal alcohol exposure and IQ at age 8: evidence from a population-based birth-cohort study. SPME–GC/MS is a simple, fast and sensitive method for the routine analysis of ethanol in food. For fish stew cooked for 45 min in a covered pan where the wine was added in cold ingredients, alcohol retention was 30%, whereas for beef bib and hunter rabbit with red wine added to boiling ingredients and then cooked for 1 h in a covered pan the ethanol retention was 5%. The limits of quantification were registered at levels of parts per million. Correspondence to J Chromatogr B Anal Technol Biomed Life Sci 773:75–82, Wasfi IA, Al-Awadhi AH, Al-Hatali ZN, Al-Rayami FJ, Al Katheeri NA (2004) Rapid and sensitive static headspace gas chromatography–mass spectrometry method for the analysis of ethanol and abused inhalants in blood. Both liquids require the addition of some other chemical or contamination of some sort. Copyright © 2020 Elsevier B.V. or its licensors or contributors. Baseline levels of acetaldehyde, acetone, methanol and ethanol could be measured in patients before dosing commenced and an increase in levels of some volatiles were observed in several neonates after receiving ethanol-containing medications. The limits of quantification were registered at levels of parts per million. https://doi.org/10.1016/j.foodchem.2010.11.117. Calibration curves that were constructed for ethanol spiked into blank samples followed linear relationships with highly significant (p < 0.001) correlation coefficients (r > 0.999). CAS  Copyright © 2010 Elsevier Ltd. All rights reserved. - 192.232.239.125. Learn more about Institutional subscriptions, Ziavrou K, Boumba VA, Vougiouklakis TG (2005) Insights into the origin of postmortem ethanol. Labmedicine 39:42–45, De Martinis BS, Ruzzene MAM, Martin CCS (2004) Determination of ethanol in human blood and urine by automated headspace solid-phase microextraction and capillary gas chromatography. Ethanol has been part of alcoholic beverages for long time, but its application has expanded much beyond that during the 20th Century. https://doi.org/10.1007/s00216-013-6809-1, DOI: https://doi.org/10.1007/s00216-013-6809-1, Over 10 million scientific documents at your fingertips, Not logged in A fibre coated with 75 μm CAR/PDMS film was chosen to extract the ethanol. Arch Dis Child Fetal Neonatal Ed 94:F236–F240, Shehab N, Lewis CL, Streetman DD, Donn SM (2009) Exposure to the pharmaceutical excipients benzyl alcohol and propylene glycol among critically ill neonates. The conditions selected for HS-SPME–GC/MS demonstrated that the technique has high linearity and reproducibility. PubMed Google Scholar. Clin Chem 22:802–805, Pontes H, de Pinho PG, Casal S, Carmo H, Santos A, Magalhaes T, Remiao F, Carvalho F, Bastos ML (2009) GC determination of acetone, acetaldehyde, ethanol, and methanol in biological matrices and cell culture. 2 > 0.99) and the limits of detection were 0.1–0.2 mg/L and lower limits quantification 0.5–1 mg/L. ► Potential hazards of intake of meals cooked with alcoholic drinks by ethanol sensible individuals. Part of Springer Nature. Department of Chemistry, University of Leicester, Leicester, LE1 7RH, UK, Department of Infection Immunity and Inflammation, University of Leicester, Leicester, LE1 7RH, UK, Neonatal Unit, University Hospitals Leicester, Leicester, LE1 5WW, UK, Division of Perinatal and Developmental Medicine, University of Liverpool, Liverpool, L69 3BX, UK, You can also search for this author in Forensic Sci Int 165:10–29, De Martinis BS, Martin CC (2002) Automated headspace solid-phase microextraction and capillary gas chromatography analysis of ethanol in postmortem specimens. https://doi.org/10.1007/s00216-013-6809-1. Prediction of ethanol content of meals cooked with alcoholic drinks is possible for each type of cooked meals through knowledge of the initial amount of ethanol in ingredients. Dean et al. Int J Pharm 155:1–5, Pifferi G, Restani P (2003) The safety of pharmaceutical excipients. This is a preview of subscription content, log in to check access. Cordell, R.L., Pandya, H., Hubbard, M. et al. Med Sci Law 43:241–247, Kristoffersen L, Stormyhr L-E, Smith-Kielland A (2006) Headspace gas chromatographic determination of ethanol: the use of factorial design to study effects of blood storage and headspace conditions on ethanol stability and acetaldehyde formation in whole blood and plasma. (2) developed a sensitive and specific method Much of the recent interest is in the use of ethanol as fuel. The use of dealcoholised wine evaluated as a tasty alternative to the above mentioned groups. These results indicate that care must be taken with meals cooked with alcoholic drinks since they can be consumed by the paediatric age group, abstinent alcoholics, or ethanol sensible individuals. GC-MS analysis of ethanol and other volatile compounds in micro-volume blood samples—quantifying neonatal exposure. These results indicate that care must be taken with meals cooked with alcoholic drinks since they can be consumed by the paediatric age group, abstinent alcoholics, or ethanol sensible individuals. J Chromatogr A 1252:23–30, Ashley DL, Bonin MA, Cardinali FL, McCraw JM, Holler JS, Needham LL, Patterson DG Jr (1992) Determining volatile organic compounds in human blood from a large sample population by using purge and trap gas chromatography/mass spectrometry. Copyright © 2010 Elsevier Ltd. All rights reserved. The method used for sample preparation was simple. Clin Chem 38:743–747, Keim ME, Bartfield JM, Raccio-Robak N, Abhyankar VV, Salluzzo RF (1999) Accuracy of an enzymatic assay device for serum ethanol measurement. Whereas standard addition method was used for quantification of ethanol in hunter rabbit, marinated grilled steak and industrial products that refer ethanol in the ingredients. We use cookies to help provide and enhance our service and tailor content and ads. A headspace SPME method in combination with GC/MS was used for the extraction, identification, and quantification of ethanol. Il Farmaco 58:541–550, Osterberg RE, See NA (2003) Toxicity of excipients—a food and drug administration perspective. The method was applied to analyse blood samples from neonatal patients receiving courses of ethanol excipient containing medications. PLoS One 7:e49407. ► Use of dealcoholised wine as a tasty alternative to the above mentioned groups. ► Recommendations of intake of meals cooked with alcoholic drinks by pediatric age group and abstinent alcoholics. Quantification of ethanol was successfully performed in fish stew and beef bib by external standard method. We use cookies to help provide and enhance our service and tailor content and ads. Copyright © 2020 Elsevier B.V. or its licensors or contributors. ► Prediction of ethanol content of meals cooked with alcoholic drinks. Anal Bioanal Chem 405, 4139–4147 (2013). Calibration curves that were constructed for ethanol spiked into blank samples followed linear relationships with highly significant (p < 0.001) correlation coefficients (r > 0.999).

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